Process for production of aqueous solutions of free hydroxylamin

Distillation: processes – separatory – Plural distillations performed on same material – One a distillation under positive pressure or vacuum

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203 6, 203 12, 203 79, 203 80, 203 92, 203 93, 203 94, 203 96, 203 97, 203 98, 203 99, 203DIG19, 423387, B01D 338, C01B 2114

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active

058371079

ABSTRACT:
An aqueous solution of free hydroxylamine is prepared by a process in which the solution obtained by treating a hydroxylammonium salt with a base is separated into an aqueous hydroxylamine solution and a salt fraction by treatment with water or steam at .ltoreq.80.degree.0 C. The novel process can be carried out in a simple and gentle manner and on a large industrial scale. Owing to the low thermal load, the low concentration of hydroxylamine and the short residence time in the process, the risk of decomposition is minimized.

REFERENCES:
patent: 4956168 (1990-09-01), Wagaman
patent: 5266290 (1993-11-01), Levinthal et al.
patent: 5472679 (1995-12-01), Levinthal et al.
patent: 5510097 (1996-04-01), Cawlfield et al.

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