Method for producing CF.sub.3 I

Details Method for producing CF.sub.3 I Method for producing CF.sub.3 I

1988-05-19

1990-05-01

Doll, John

Organic compounds -- part of the class 532-570 series

Organic compounds

Halogen containing

570140, 570142, C07C 1720, C07C 1722

Patent

active

049220411

ABSTRACT:
A method for producing trifluoroiodomethane in which a metal Mt selected from the group magnesium, zinc, cadmium, bismuth and tin is reacted in a first step (a) with a trifluorohalomethane, and the resulting reaction mixture is further reacted in a second step (b) with a component containing iodine to produce CF.sub.3 I. Compounds corresponding to the formula CF.sub.3.Zn.X.nL are also described.

REFERENCES:
patent: 4701569 (1987-10-01), Francese et al.
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Henne et al., J. Am. Chem. Soc., "The Degradation of Silver Trifluoroacetate . . . ", 72 pages, 3806-3807, (1950).
Emeleus et al., J. Chem. Soc., "Organometallic Fluorine Compounds", pp. 2953-2956, (1949).
Habeeb et al., J. Org. Chem. 195, "The Electrochemical Synthesis of Neutral and Anionic . . . ", pp. 117-127, (1980).
Hazeldine, J. Chem. Soc., pp. 1273-1275, 1954.
McBee et al., J. Org. Chem., vol. 28, pp. 1131-1132, 1963.
Blancou et al., J.C.S. Chem. Comm., pp. 885-886, 1976.
Burton et al., J. Am. Chem. Soc., vol. 107, pp. 5014-5015, 1985.

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