Catalyst for anthraquinone hydrogen peroxide process

Catalyst – solid sorbent – or support therefor: product or process – Catalyst or precursor therefor – Silicon containing or process of making

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Details

423588, 502262, B01J 2906, B01J 2912

Patent

active

045215316

ABSTRACT:
A palladium-on-silica catalyst for the anthraquinone-hydroquinone method of preparing hydrogen peroxide is prepared by adding acid solutions of a palladium compound and of an additive metal salt to an aqueous slurry of silica particles, lowering the pH of the slurry to about 0.8-1.0, then incrementally raising the pH of the slurry to 2.3-2.7, to 3.8-4.2, then to 6.8-7.2, and then reducing the palladium compound to palladium metal.

REFERENCES:
patent: 4240933 (1980-12-01), Copelin

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