Method and apparatus for determining organic carbon in sulfureou

Chemistry: physical processes – Physical processes – Crystallization

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23253PC, G01N 3112

Patent

active

040532810

ABSTRACT:
Measured sample quantities of sulfureous matter are introduced into a sealed chamber where the samples are pyrolyzed to form sulfur dioxide and sulfur trioxide gases and to oxidize organic substances to form carbon dioxide gas. The gases are then passed through a free sulfur-absorbing packing and into a scrubbing zone wherein transition metal amine complex is used to remove sulfureous compounds without reaction with the carbon dioxide gas. The scrubbed gases are then analyzed to determine the carbon dioxide content thereof.

REFERENCES:
patent: 2736638 (1956-02-01), McConnaughey
patent: 3346342 (1967-10-01), Miller
patent: 3451779 (1969-06-01), Hozumi
patent: 3698869 (1972-10-01), Condon
patent: 3753656 (1973-08-01), Matson et al.
patent: 3762878 (1973-10-01), Villalobos
patent: 3861874 (1975-01-01), Krc
Aloe Scientific Catalog 103; 1952; p. 1010.
Merck Index 7th ed., 1960, p. 303.

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