Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...
Patent
1985-11-01
1987-05-26
Jiles, Henry R.
Organic compounds -- part of the class 532-570 series
Organic compounds
Heterocyclic carbon compounds containing a hetero ring...
C07D23334
Patent
active
046687939
ABSTRACT:
A process for producing 1,3-dimethyl-2-imidazolidinone with a high yield which comprises reacting N,N'-dimethylethylene diamine and/or its hydrochloride with phosgene in the presence of a substantial amount of water and a dehydrochlorinating agent. Particularly, higher yield is attained by carrying out the reaction in water medium while controlling a pH to the range of 3.0 to 10.0 by adding a dehydrochlorinating agent.
REFERENCES:
Puschin et al. Compounds of Phosgene with Hexamethylenetetramine, m-Toluidine and Ethylenediamine.
Kajimoto Nobuyuki
Nagata Teruyuki
Nakayama Hitoshi
Wada Masaru
Yamada Tadao
Jiles Henry R.
Mitsui Toatsu Chemicals Inc.
Richter J.
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