Process for the preparation of 3-cyano-3,5,5-trimethylcyclohexan

Organic compounds -- part of the class 532-570 series – Organic compounds – Nitriles

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558431, C07C25310

Patent

active

050119680

ABSTRACT:
A process for preparing isophorone nitrile is disclosed, whereby isophorone is reacted with hydrogen cyanide in the presence of a quaternary ammonium catalyst. Remaining catalyst is removed by thermal destruction and nitrogen sparging. Residual cyanide is removed by acidification and nitrogen sparging.

REFERENCES:
patent: 4299775 (1981-11-01), Dubreux
Chemical Abstracts 60:11885e (1964), Musker.
Chemical Abstracts 103:75809z (1985), Sumitomo.

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