Process for preparing dimethyl .beta.,.beta.-dichlorovinylphosph

Details Process for preparing dimethyl .beta.,.beta.-dichlorovinylphosph Process for preparing dimethyl .beta.,.beta.-dichlorovinylphosph

1982-06-21

1984-08-07

Sutto, Anton H.

Chemistry of carbon compounds

Dipeptides, e.g., aspartame, anserine, carnosine, etc.

260956, C07F 940

Patent

active

044643080

ABSTRACT:
A process for preparing dimethyl .beta.,.beta.-dichlorovinylphosphate is provided by reaction of chloral with trimethylphosphite at atmospheric pressure, wherein, for completing the reaction, the reaction mixture is heated at a temperature of 150.degree.-210.degree. C. during at least 10 seconds.

REFERENCES:
patent: 2765331 (1956-10-01), Whetstone et al.
patent: 2956073 (1960-10-01), Whetstone et al.
patent: 3116201 (1963-12-01), Whetstone et al.

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