Process for the production of orotic acid

Details Process for the production of orotic acid Process for the production of orotic acid

1976-08-11

1977-12-20

Coughlan, Jr., Paul M.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D23954

Patent

active

040641260

ABSTRACT:
A process for the trichloroacetyl of orotic acid which comprises (a) converting trichloroacetyl chloride to .gamma., .gamma., .gamma.-trichloroacetoacetyl chloride with ketene, (b) adding reaction mixture (a) to urea dissolved in a polar organic solvent, e.g., acetic acid, 6-trichloromethyluracil being produced, (c) separating the 6-trichloromethyluracil from reaction mixture (b), and (d) hydrolyzing the 6-trichloromethyluracil to orotic acid.

REFERENCES:
patent: 3838128 (1974-09-01), Lutz et al.

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