Preparation of 5-methyl-2-nitrophenol

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07C 7924

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040340503

ABSTRACT:
Process for preparing 5-methyl-2-nitrophenol of high purity by sulfonating tri-m-cresyl phosphate, nitrating the sulfonated tri-m-cresyl phosphate, hydrolyzing the nitrated, sulfonated tri-m-cresyl phosphate to obtain a mixture of nitro-m-cresols, steam-distilling the mixture, and repeatedly washing the distillate with a dilute aqueous alkaline solution.

REFERENCES:
patent: 2810767 (1957-10-01), Clarke
patent: 2985688 (1961-05-01), Mersch et al.

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