Process for preparing alkyl nitroacetates

Details Process for preparing alkyl nitroacetates Process for preparing alkyl nitroacetates

1982-11-04

1985-01-22

Shippen, Michael L.

Organic compounds -- part of the class 532-570 series

Organic compounds

Carboxylic acid esters

560 21, 560 22, 560156, 260404, C07C 7941, C07C 7942, C07C 7946

Patent

active

044953623

ABSTRACT:
A process for preparing alkyl nitroacetates by reacting an alkyl phenyl carbonate with a nitroparaffin in a polar aprotic solvent in the presence of a cyanide ion. The process permits a higher reaction rate, and thus the reaction can be completed even at room temperature.

REFERENCES:
Allinger, "Organic Chemistry," p. 25, (1971).

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