Process for making thiobiscarbamates

Details Process for making thiobiscarbamates Process for making thiobiscarbamates

1982-04-15

1985-01-22

Jiles, Henry R.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C10312

Patent

active

044950934

ABSTRACT:
An improved method for the preparation of stable, thiobiscarbamates in high yields and high purity is provided which involves the in situ reaction of a carbamate with a sulfur chloride in the presence of a nitrogen-containing heterocyclic base and thereafter quenching and washing the reaction slurry with an alcohol at low temperatures.

REFERENCES:
patent: 4323516 (1982-04-01), Ashworth et al.
Conrow & McDonald, Deductive Organic Chemistry, Addison-Wesley Pub. Co., Inc. Reading Mass., 1966, p. 116.

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