Process for making aryl chloromethyl sulfides

Details Process for making aryl chloromethyl sulfides Process for making aryl chloromethyl sulfides

1975-01-17

1977-03-29

Rizzo, Nicholas S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260302A, 260302S, 260306, 2603096, 2602948G, 260307D, 260283S, 260556AR, 260609E, 260609F, C07C14800, C07C14934, C07D27736

Patent

active

040148912

ABSTRACT:
The title compounds are prepared in excellent yields by reacting an alkali aromatic mercaptide with bromochloromethane in the presence of a quaternary ammonium salt having ten or more carbon atoms. Normally the chlorobromomethane is used in excess as the liquid reaction medium. Reaction temperatures are normally selected in the range of from about 20.degree. to about 65.degree. C.

REFERENCES:
patent: 2776977 (1957-01-01), D'Amico
patent: 3669981 (1972-06-01), Pera et al.
Babayan et al., Chemical Abstracts, vol. 55, 11342g (1961).
Herriott, Synthesis, p. 447 (July 1975).

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