Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof
Patent
1992-05-21
1993-04-06
Tsang, Cecilia
Organic compounds -- part of the class 532-570 series
Organic compounds
Carboxylic acids and salts thereof
549246, 562483, C07D30789, C07C 5106
Patent
active
052005569
ABSTRACT:
Process for the preparation of 3,4,6-tetrafluorophthalic acid of the formula (1) ##STR1## or the anhydride thereof in good yields and in an advantageous manner, by dehalogenating tetrafluorophthalic anhydride of the formula (2) ##STR2## or tetrafluorophthalic acid in aqueous-alkaline medium using zinc at temperatures of approximately 20.degree. C. to approximately 160.degree. C. and, if appropriate, converting the resulting 3,4,6-trifluorophthalic acid into the anhydride in a known manner by dehydrating it.
REFERENCES:
patent: 1935648 (1933-11-01), Mares
patent: 2460564 (1949-02-01), Amacker
patent: 3007943 (1961-11-01), Hoffmann
patent: 3092641 (1963-06-01), Leon
patent: 3240792 (1966-03-01), Patrick et al.
patent: 4302396 (1981-11-01), Tsujimoto et al.
patent: 4814467 (1987-03-01), Bay et al.
patent: 4962206 (1990-10-01), Coceman et al.
patent: 5086188 (1992-02-01), Fertel et al.
Hashem, J. Appl. Chem. Biotechnol (1972) 22, 1041-1042.
Delbridge, T. G., Am. Chem. J. 41:393, 400-409 (1909).
O'Reilly, N. J., et al. Synlet:339-340, Jun. 1990.
O'Reilly, N. J., et al, Synlet:609-610, Oct. 1990.
Papenfuhs Theodor
Pfirmann Ralf
Hoechst Aktiengesellschaft
Tsang Cecilia
LandOfFree
Process for the preparation of 3,4,6-trifluorophthalic acid and does not yet have a rating. At this time, there are no reviews or comments for this patent.
If you have personal experience with Process for the preparation of 3,4,6-trifluorophthalic acid and , we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for the preparation of 3,4,6-trifluorophthalic acid and will most certainly appreciate the feedback.
Profile ID: LFUS-PAI-O-538025