Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof
Patent
1982-09-29
1985-02-26
Killos, Paul J.
Organic compounds -- part of the class 532-570 series
Organic compounds
Carboxylic acids and salts thereof
560 64, C07C 6500, C07C 6976
Patent
active
045019207
ABSTRACT:
A salt of 3,4,5-trimethoxybenzoic acid is prepared by initially reacting hydrolyzable tannin with a methylation agent in an alkaline medium under methylation conditions to form methylated tannin and thereafter hydrolyzing the methylated tannin by reaction thereof with a hydrolysis agent under alkaline hydrolysis conditions. The resulting salt can be neutralized to form 3,4,5-trimethoxybenzoic acid, which can readily be recovered.
REFERENCES:
Kutani, N. Chem. Pharm. Bull., vol. 8, pp. 72-76, 1960.
Britton et al., J. Chem. Soc., 1966, pp. 783-790.
Goodwin L. N.
Jackson R. G.
Killos Paul J.
Klostermann R. J.
Mallinckrodt Inc.
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