Preparation of nitroalcohols

Details Preparation of nitroalcohols Preparation of nitroalcohols

1983-07-08

1985-01-29

Lone, Werren B.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568876, C07C 7918

Patent

active

044967721

ABSTRACT:
In a process for preparing a nitroalcohol by reacting a nitroparaffin and an aldehyde in a solvent, the improvement comprising the use of 0.5 to 5 mole percent of a trialkyl phosphine, based on the nitroparaffin, which greatly reduces reaction time to 0.1 to 5 hours.

REFERENCES:
patent: 3534112 (1970-10-01), Tindall
patent: 3564062 (1971-02-01), Tindall
patent: 3723546 (1973-03-01), Bachmen et al.
patent: 4241226 (1980-12-01), Adrain et al.
Vanderbilt et al, "Industrial and Eng. Chem.", vol. 32, (1940), TP1A54, pp. 34-38.

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