Process for the production of thiotetronic acid

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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C07D33336

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049979574

ABSTRACT:
Process for the production of thiotetronic acid wherein 4-chloroacetoacetic acid chloride is reacted with hydrogen sulfide in the presence of an amine.

REFERENCES:
patent: 2453103 (1944-02-01), Turnbull
Chemical Reviews, vol. 86, No. 2 (Apr. 1986), pp. 245 and 246.
D. B. Macierewicz, Rocz. Chem. 47, (1973), p. 1735.
J. Z. Mortensen et al., Tetrahedron 27 (1971), p. 3839.
Wang et al., Tetrahedron Letters, vol. 25, No. 46, pp. 5243-5246 (1984).
E. Benary, Chemische Berichte 46 (1913), pp. 2103 and 2107.
Turnbull, Chem. Abst., vol. 43, (1949), p. 2238.
Chem. Abst., vol. 78, (1973), 29615a.

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