Selective preparation of cis-perhydroacenaphthene

Details Selective preparation of cis-perhydroacenaphthene Selective preparation of cis-perhydroacenaphthene

1987-05-04

1988-11-08

Garvin, Patrick P.

Chemistry of hydrocarbon compounds

Adding hydrogen to unsaturated bond of hydrocarbon, i.e.,...

Hydrocarbon is aromatic

585266, 585267, 585269, C07C 510

Patent

active

047835656

ABSTRACT:
A cis-isomer of perhydroacenaphthene is selectively prepared through hydrogenation of acenaphthene by effecting hydrogenation of 80.degree. to 200.degree. C. in the presence of a Ru and/or Rh based catalyst. A cis-isomer having the highest boiling point is obtained as a major product.

REFERENCES:
patent: 3128316 (1964-04-01), Schneider
patent: 3183278 (1965-05-01), Koch
patent: 3349140 (1967-10-01), Weitkamp
patent: 4046824 (1977-09-01), Ransley
patent: 4329529 (1982-05-01), Nambu
"Preparation of Diamondoid Hydrocarbons by Rearrangement Employing a Chlorinated Platinum-Alumina Catalyst", Journal of the American Chemical Society, by D. E. Johnston et al., Jun. 2, 1971, pp. 2798 and 2799.

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