Preparation of yttria-stabilized zirconia reaction sintered...

Plastic and nonmetallic article shaping or treating: processes – Outside of mold sintering or vitrifying of shaped inorganic... – Of electrical article or electrical component

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C501S103000, C501S152000

Reexamination Certificate

active

07833469

ABSTRACT:
A method of making a solid electrolyte-YSZ product, where the method includes the step of providing a powdered mixture of zirconia, yttria and about 2%, by wt., or less of a metal oxide, where yttria-stabilized zirconia is not added to the mixture. The method also includes sintering the powdered mixture at about 1500° C. or less, for about 5 hours or less, to form a reaction sintered YSZ. Also, a method of making a fuel cell electrolyte that includes the step of forming a green body that includes zirconia, yttria and about 2%, by wt., or less of a metal oxide, where yttria-stabilized zirconia is not added to the green body. The method also includes shaping the green body into a form of the electrolyte, and sintering the green body at about 1500° C. or less to form a reaction sintered yttria-stabilized zirconia and metal oxide electrolyte.

REFERENCES:
patent: 3300344 (1967-01-01), Bray et al.
patent: 3503809 (1970-03-01), Spacil
patent: 3558360 (1971-01-01), Sverdrup et al
patent: 3607323 (1971-09-01), Tedmon et al.
patent: 4465778 (1984-08-01), Brook et al.
patent: 4767518 (1988-08-01), Makalick
patent: 4866014 (1989-09-01), Cassidy et al.
patent: 4883497 (1989-11-01), Claar et al.
patent: 4971830 (1990-11-01), Jensen
patent: 5035962 (1991-07-01), Jensen
patent: 5118491 (1992-06-01), Castellano et al.
patent: 5217822 (1993-06-01), Yoshida et al.
patent: 5227258 (1993-07-01), Ito et al.
patent: 5261944 (1993-11-01), Lockhart et al.
patent: 5368667 (1994-11-01), Minh et al.
patent: 5474800 (1995-12-01), Matsuzaki
patent: 5543239 (1996-08-01), Virkar et al.
patent: 5589017 (1996-12-01), Minh
patent: 5656387 (1997-08-01), Barnett et al.
patent: 5788788 (1998-08-01), Minh
patent: 5804131 (1998-09-01), Majumdar et al.
patent: 5908713 (1999-06-01), Ruka et al.
patent: 5993511 (1999-11-01), Piro et al.
patent: 6099985 (2000-08-01), Elangovan et al.
patent: 6248468 (2001-06-01), Ruka et al.
patent: 6312847 (2001-11-01), Tsukuda et al.
patent: 6344426 (2002-02-01), Hata et al.
patent: 6379417 (2002-04-01), Piro et al.
patent: 6432570 (2002-08-01), Ippommatsu et al.
patent: 6589680 (2003-07-01), Gorte et al.
patent: 6692855 (2004-02-01), Aizawa et al.
patent: 6790474 (2004-09-01), Hishinuma et al.
patent: 7045231 (2006-05-01), Coors
patent: 7527761 (2009-05-01), Swartzlander et al.
patent: 2003/0219637 (2003-11-01), Coors
patent: 2003/0224240 (2003-12-01), Yamashita et al.
patent: 2006/0125157 (2006-06-01), Swartzlander et al.
PCT International Search Report and Written Opinion mailed Oct. 1, 2008, International Application No. PCT/US2008/050748, 15 pages.
Anselmi-Tamburini, U. et al., “Electrical Properties Of Ni/YSZ Cermets Obtained Through Combustion Synthesis,” Solid State Ionics, vol. 110, pp. 35-43, 1998.
Chen, S. et al., “Effect Of NiO Dissolution On The Transformation Of Plasma-Sprayed Y-PSZ,” Materials Science and Engineering, vol. A114, pp. 159-165, 1989.
Chen, Shueiyuan et al., “Growth Kientics Of Sintered NiO/ZrO2 (5 mol.% Y2O3) Composites,” Materials Science and Engineering, vol. A158, pp. 251-258, 1992.
Chen, Shueiyuan et al., “Polymorphic Transformation Of t′ Phase In Yttria Partially Stabilized Zirconia,” Materials Science and Engineering, vol. A123, pp. 145-152, 1990.
Chen, Shueiyuan et al., “Stability of Cubic ZrO2 (10 mol.% Y2O3) When Alloyed With NiO, Al2O3 Or TiO2: Implications To Solid Electrolytes And Cermets,” Materials Science and Engineering, vol. B22, pp. 247-255, 1994.
Kuzjukevics, A. et al., “Plasma Produced Ultrafine YSZ-NiO Powders,” Proceedings of the 17th Riso International Symposium on Materials Science, Roskilde, Denmark, pp. 319-324, 1996.
Linderoth, Soren et al., “NiO In Yttria-Doped Zirconia,” Proceedings of the Fifth International Symposium on Solid Oxide Fuel Cells (SOFC-V), vol. 97-40, pp. 2 cover pages and 1076-1085, 1997.
Marinsek, Marjan et al., “Ni-YSZ Cermet Anodes Prepared by Citrate/Nitrate Combustion Synthesis”, J. Power Sources 106 (2002), pp. 178-188.
Marinsek, Marjan et al., “Preparation of Ni-YSZ Composite Materials for Solid Oxide Fuel Cell Anodes by the Gel-Precipitation Method”, J. Power Sources 86 (2000), pp. 383-389.
Primdahl, Soren et al., “Effect of Nickel Oxide/Yttria-Stabilized Zirconia Anode Precursor Sintering Temperature On The Properties Of Solid Oxide Fuel Cells,” J. Am. Ceram. Soc., vol. 83, No. 3, pp. 489-494.
Ringuede, A. et al., “A Combustion Synthesis Method To Obtain Alternative Cermet Materials For SOFC Anodes,” Solid State Ionics, vols. 141-142, pp. 549-557, 2001.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Preparation of yttria-stabilized zirconia reaction sintered... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Preparation of yttria-stabilized zirconia reaction sintered..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Preparation of yttria-stabilized zirconia reaction sintered... will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-4191506

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.