Amine catalysts for the low temperature conversion of silica pre

Coating processes – With post-treatment of coating or coating material – Chemical agent applied to treat coating

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4271262, 4271264, 427226, 427344, 427377, 427387, 4273977, B05D 304, B05D 310

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active

051166372

ABSTRACT:
This invention relates to a low temperature method of converting coatings of hydrogen silsesquioxane resin or hydrolyzed or partially hydrolyzed R.sub.X Si(OR).sub.4-X to ceramic silica coatings. The method comprises applying a silica precursor coating to a substrate, exposing the coating to an environment comprising an amine and subjecting the coating to a temperature sufficient to yield the ceramic coating. The methods of the invention are particularly applicable to applying coatings on electronic devices.

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W. Noll, "Chemistry & Technology of Silicones", Academic Press, NY, N.Y. (1968), pp. 205, 213.
R. L. Merker, et al., J Polymer Science-Part A, vol. 2, pp. 31-44 (1964).
J. of Non-Crystalline Solids, 64, 209-221 (1984).

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