Ethanol extraction of phytosterols from corn fiber

Drug – bio-affecting and body treating compositions – Designated organic active ingredient containing – Cyclopentanohydrophenanthrene ring system doai

Reexamination Certificate

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C514S169000, C514S054000, C514S057000, C514S060000, C536S005000, C424S750000, C426S482000

Reexamination Certificate

active

07833994

ABSTRACT:
The present invention provides a process for extracting sterols from a high solids, thermochemically hydrolyzed corn fiber using ethanol as the extractant. The process includes obtaining a corn fiber slurry having a moisture content from about 20 weight percent to about 50 weight percent solids (high solids content), thermochemically processing the corn fiber slurry having high solids content of 20 to 50% to produce a hydrolyzed corn fiber slurry, dewatering the hydrolyzed corn fiber slurry to achieve a residual corn fiber having a moisture content from about 30 to 80 weight percent solids, washing the residual corn fiber, dewatering the washed, hydrolyzed corn fiber slurry to achieve a residual corn fiber having a moisture content from about 30 to 80 weight percent solids, and extracting the residual corn fiber with ethanol and separating at least one sterol.

REFERENCES:
patent: 5776535 (1998-07-01), Palardy
patent: 5843499 (1998-12-01), Moreau
patent: 2001/0020091 (2001-09-01), Buchanan et al.
patent: 2003/0235633 (2003-12-01), Abbas et al.
patent: 00/47701 (2000-08-01), None
Singh et al. (Cereal Chemistry (2003), 80 (2), 118-122) (Abstract Sent).
Supplementary European Search Report dated July 10, 2009.
Moreau et al. “Phytosterols in the Aleurone Layer of Corn Kernals”, Biochemical Society Transactions, vol. 28, No. 6, Dec. 2000, pp. 803-806.

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