Process for producing niobium and tantalum compounds

Chemistry of inorganic compounds – Oxygen or compound thereof – Metal containing

Reexamination Certificate

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Reexamination Certificate

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11142066

ABSTRACT:
A process for producing valve metal oxides, such as tantalum pentoxide or niobium pentoxide with a narrow particle size distribution within a desired particle size range, is provided. According to the process of the present invention, the valve metal fraction from digestion of valve metal material containing ore is processed under controlled temperature, pH, and residence time conditions to produce the valve metal pentoxide and pentoxide hydrates. Also, disclosed are new tantalum pentoxide and niobium pentoxide products and new tantalum pentoxide precursors and niobium pentoxide precursors.

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D13: Annex to Substantiation of Appeal regarding EP 854841, graph (with full English translation).
Hervieu et al., “Ion Exchange Properties of Some Pyrochore Type Ternary Oxides: the Pyrochores H1+x(H2O)Ta1+xO6and NH4TaWO6”, UER Sciences, Universite de Caen, Esplanade de la Paiz, 14-Caen, Jun. 9, 1971 (with full English translation).
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D3D: Delivery Note—Kyocera K.K. (with translation), no date.
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D5D: 2 Purchase Orders Asahi Kogaku Kogyo (with translation), no date.
D5E: Invoice Asahi Kogaku Kogyo (with translation), no date.
D5F: Invoice Asahi Kogaku Kogyo (with translation), no date.
Invoice Asahi Kogaku Kogyo (with translation), no date.
D5H: Inspection Certificate Asahi Optical, no date.
D5K: Dispatch Note Asahi Optical, Jun. 16, 1993.
D5L: Invoice H.C. Starck Japan, Jun. 15, 1993.
D5M: Invoice H.C. Starck Japan, Jun. 15, 1993.
D5N: Dispatch Note Asahi Optical, Jun. 16, 1993.
D5O: Inspection Certificate Asahi Optical, Jun. 10, 1993.
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D12: Experimental Data Ta2O5/Nb2O5Precipitations according to EP 0854841 B1 (with translation), no date.

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