Process for preparing organic hydroperoxide having a reduced...

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

Reexamination Certificate

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C549S542000, C568S754000, C208S25100H, C208S25100H

Reexamination Certificate

active

07067680

ABSTRACT:
A process for preparing organic hydroperoxide having a reduced content of contaminants, which process involves:(a) oxidation of an organic compound to obtain reaction product containing an organic hydroperoxide;(b) contacting at least part of the organic hydroperoxide containing reaction product with a basic aqueous solution;(c) separating the hydrocarbonaceous phase containing organic hydroperoxide from the aqueous phase;(d) washing at least part of the separated hydrocarbonaceous phase containing organic hydroperoxide; and(e) contacting at least part of the hydrocarbonaceous phase containing organic hydroperoxide with a guard bed having solid adsorbent with a void content of from 50% to 98% by volume.

REFERENCES:
patent: 4539101 (1985-09-01), Oleck et al.
patent: 4601998 (1986-07-01), Oleck et al.
patent: 5723637 (1998-03-01), Tsuji et al.
patent: 5883268 (1999-03-01), Lin et al.
patent: 0 345 856 (1989-12-01), None
patent: 99/42425 (1999-08-01), None
patent: 99/42426 (1999-08-01), None
International Search Report dated Jul. 5, 2002.

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