Organic compounds -- part of the class 532-570 series – Organic compounds – Isocyanate esters
Reexamination Certificate
2006-03-28
2006-03-28
Richter, Johann (Department: 1621)
Organic compounds -- part of the class 532-570 series
Organic compounds
Isocyanate esters
C560S336000
Reexamination Certificate
active
07019164
ABSTRACT:
The present invention relates to a process for the production of an isocyanate corresponding to the formula R(NCO)nwhereinR represents a (cyclo)aliphatic or aromatic hydrocarbon residue having up to 15 carbon atoms, preferably 4 to 13 carbon atoms, provided that there are at least 2 carbon atoms arranged between each of the nitrogens andn represents the number 2 or 3,bya) separately heating an amine corresponding to the formula R(NH2)n, wherein R and n are as previously defined, in vapor form, optionally diluted with an inert gas or the vapors of an inert solvent, and phosgene to temperatures of 200° C. to 600° C.,b) continuously reacting the optionally diluted amine and phosgene in a reactor which has a reaction chamber that does not have moving parts, wherein the reactor has a diameter D and centrally located in the reactor is a nozzle having an orifice diameter d,i) by introducing the optionally diluted amine into the reactor through the nozzle and by introducing phosgene through the annular space around the nozzle such that the amine and phosgene flow in parallel through the reactor andii) mixing and reacting the amine and phosgene to form the isocyanate of formula I) by introducing the amine through the orifice into a stream of phosgene in the reaction chamber,wherein the gas velocity of the optionally diluted amine is higher than the gas velocity of phosgene and the ratio of the narrower nozzle diameter d to the reactor diameter D is from 5% to 45%.
REFERENCES:
patent: 4847408 (1989-07-01), Frosch et al.
patent: 5391683 (1995-02-01), Joulak et al.
patent: 5449818 (1995-09-01), Biskup et al.
patent: 5516935 (1996-05-01), Bischof et al.
patent: 5633396 (1997-05-01), Bischof et al.
patent: 6100326 (2000-08-01), Richter et al.
patent: 2003/0069441 (2003-04-01), Leimkuhler et al.
Friedrich Martin
Stutz Herbert
Bayer Aktiengesellschaft
Gil Joseph C.
Puttlitz Karl
Richter Johann
Roy Thomas W.
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