Polyoxyalkylene monoalkyl ether, process for producing the...

Cleaning compositions for solid surfaces – auxiliary compositions – Cleaning compositions or processes of preparing – Liquid composition

Reexamination Certificate

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C510S434000, C510S475000, C510S477000, C510S535000, C568S616000, C568S618000, C560S183000, C560S186000, C560S187000, C524S599000, C528S271000, C528S272000, C528S306000, C528S392000

Reexamination Certificate

active

06956018

ABSTRACT:
A polymerizable polyoxyalkylene monoalkyl ether derivative prepared by using a polyoxyalklene monoalkyl ether which gives, in gel permeation chromatography, a chromatogram which satisfies a relation expressed by an equation: S1/S0≦0.15, wherein S1represents the area under a portion of the chromatogram from the start of elution to the earliest elution time when the intensity of the refractive index has a value of L/3, L representing the shortest distance between the greatest maximum point of the intensity of the refractive index and the base line and S0represents the area under a portion of the chromatogram from the start of elution to an elution time when the intensity of the refractive index has the greatest maximum value; a process for producing the above ether comprising adjusting the content of water in a reactor, which is used in addition polymerization of alkylene oxides with addition to a monohydric alcohol, so as to satisfy an equation: Wi×(Cf−Ci)/V≦10, wherein the content of water in the reactor is obtained by placing a solvent having a content of water Ci (ppm) in an amount Wi (g) in the reactor having an inner volume V (ml), stirring the solvent to clean the reactor, removing the solvent from the reactor and obtaining a content of water Cf (ppm) in the removed solvent.

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Derwent Publications Ltd., London, GB, AN 1998-20170; XP002175001 & JP 10 053738 A; Feb. 24, 1998.
Derwent Publications Ltd., London, GB; AN 1982-10561J: XP002175002 & JP 57 185308 A; Nov. 15, 1982.
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