Optics: measuring and testing – For size of particles
Reexamination Certificate
2003-03-06
2004-11-23
Stafira, Michael P. (Department: 2877)
Optics: measuring and testing
For size of particles
Reexamination Certificate
active
06822736
ABSTRACT:
FIELD OF THE INVENTION
The present invention relates to a method for automatic analysis to determine particle size distribution, shape and color, and an apparatus for performing the method. The method includes a collection of particle samples, and a transportation of the collected particle samples to a means for distributing the particles into a particle stream. The means for distributing the particles forms a curtain where the particles are substantially distributed in a monolayer to be exposed to a light source for providing an image of the particle curtain to be analyzed. The apparatus comprises sample collecting devices, and a transport means for transporting the samples to a device for distribution of the samples into a particle stream suitable for imaging and subsequent analysis.
BACKGROUND OF THE INVENTION
The main problem experienced in particle analysis is that commercially available apparatuses and methods only solve separate tasks within the field. Several manual operations are necessary for carrying out the total analysis process, and accordingly, only part of the process will in practice be automatic. In most cases, only separate samples can be analyzed at any given time, and new samples have to be collected, prepared, marked/registered and formed into suitable particle streams for imaging and subsequent computerized analysis/treatment of the images. The result of these problems is that it is quite time-consuming to perform analysis of particle samples, as well as a series of samples from different production streams of a plant.
Several apparatuses and measuring/analyzing techniques related to particle analysis are known in the art. For example, a particle analysis apparatus where a silhouette projection method is used is described in U.S. Pat. No. 4,497,576. The apparatus includes use of parallel laser beams directed through a sample of particles, and a means for recording the light which has passed through. This recording is then analyzed to reveal the particle size distribution of the sample. The particles to be analyzed are transported on a conveyor belt and fall from it in front of a light source and down to a next belt to be returned to the process. The particles falling from the belt form a monolayer of particles and they fall at the same speed. How this can be achieved is not explained.
Analysis of particle size distribution is also known from EP-0348469 B1, which describes a method and means for creating a monolayer curtain of particles to be analyzed. The particles are fed manually via a silo onto a vibrating plate disposed at such a distance from the silo outlet that the uppermost layer of said particles on said plate forms an angle with the horizontal plane which is 95%-50% of the sliding angle of said particles. Though a reliable monolayer is provided with this method and means, they are restricted to analyzing single samples, one at a time. The imaging of the particle curtain has to be finalized before a new sample of particles can be fed to the apparatus for being formed into a monolayer of particles.
Imaging and analyzing of a particle stream is also known from GB-2,333,594 A, which describes an apparatus comprising electro-optical scanning of the particle stream with an optoelectronic measurement section formed by a light source and an image collecting device. The image collecting device comprises a plurality of electro-optical image recording units aligned onto the particle stream, said units having different image scales which are mutually matched to cover the overall measurement range of the apparatus. This way of covering the overall measurement range avoids the manual work of changing lenses and camera position, but it is also restricted to performing analysis of single samples, and there are no special provisions for securing a monolayer of particles to be imaged.
In U.S. Pat. No. 4,295,200 there is described an automatic particle analyzing system comprising a supply of several samples to a particle distributor. Sample cups filled with particles are fixed on to a conveyer belt which can pass over a particle distribution device. A measured stream of particles is dropped onto the apex of a distribution cone when a cup passes over the cone. The particles are then divided into a circular pattern falling through a narrow sizing zone onto the spherical edge of a rotatable platen. By this means, the particles can be analyzed one-by-one as each particle is carried into a frame area and viewed, preferably by a microscope and a TV camera, the output of which is applied to a computer programmed to analyze selected characteristics. This system makes it possible to analyze each particle in a sample, and can continue on to the next sample when the last particle of the first sample is analyzed. But such a device is very sensitive to the particle size distribution before imaging, as large particles will get stuck in the narrow sizing zone of the apparatus. Another limitation of the capacity of the system is that the particles have to be analyzed one-by-one, and the practical use of this system will be restricted to laboratories as it is not applicable for analyzing particles in a continuous industrial process.
SUMMARY OF THE INVENTION
The main object of the present invention is to arrive at a versatile and automatic method and apparatus for the analysis of a plurality of samples of particles and being applicable both for on-line analysis and laboratory analysis.
Another object is to combine sample collections from various process streams with supply of these to a single particle analyzing apparatus without applying any manual work and still being able to keep track of the origin of the samples with regard to a time and place for collection of the various samples.
A further object is to be able to perform sequential analysis of samples, for instance, analysis of samples taken at the same time from various process streams.
It is also an object to develop a method that can cover a wide range of particle size distribution, shape and color.
In spite of the fact that numerous methods and apparatuses for particle analysis are on the market, the inventors of the present invention have found that none of these, or combinations thereof, could meet their demand for a versatile and robust system. A thorough investigation of advantages and disadvantages of known methods revealed that further developments were necessary for reducing the manual work in connection with particle analysis. It was also found that quality control of such systems needed to be improved. The inventors first looked into each manual operation in order to evaluate the possibility for automation and improvement of the operation. It was found that the sampling should be combined with placement of the sampled particles in containers which could be transported to the central unit of a particle analyzer. This conclusion led to the problem of identifying the samples later on. This problem is simply solved by providing each container with identification codes (ID) which can be arranged in sample sequence in the magazine, wherein the analyzer is set up for analyzing the samples according to the sequence of the samples and/or read for recording by conventional optical/electronic registration devices. It is then possible to identify the samples throughout the whole process with regard to a time and place for the sampling and also other information of interest such as temperature, humidity etc. at the time of sampling. In some cases it is of interest to treat the samples before analyses. Such treatment, comprising drying, dividing, crushing, sieving etc., should be performed before the sample is put into the container. In connection with particle analysis, it would in some cases be an advantage if the analysis could be performed in sequences or series, for instance, performing analysis in series of samples taken at the same time from different process streams. The inventors found that this could be achieved by applying the concept of sample containers having ID's. Desired sample series can be collected i
Johnsen Ole Magne
Jørgensen Terje
Reinholt Frode
Norsk Hydro ASA
Stafira Michael P.
Wenderoth , Lind & Ponack, L.L.P.
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