Cleaning and liquid contact with solids – Processes – Including regeneration – purification – recovery or separation...
Patent
1975-07-11
1977-02-22
Bashore, S. Leon
Cleaning and liquid contact with solids
Processes
Including regeneration, purification, recovery or separation...
134 13, 134 22R, 134 38, 203 47, 203 48, 210 42R, B08B 308, B08B 310
Patent
active
040090485
ABSTRACT:
Vinyl halide polymers are removed from the internal surfaces of reaction equipment with a solvent and the solvent recovered by: (1) contacting the polymer-containing solvent with steam forming a slurry; (2) cooling the slurry to form a crumbly precipitate; (3) separating the resulting slurry into an aqueous solvent and a precipitate; (4) adding water to the precipitate to form a second slurry; and (5) separating the second slurry into a second aqueous solvent solution and vinyl halide polymers. The aqueous solvent solutions are dehydrated before being reused in solvent cleaning.
REFERENCES:
patent: 2389958 (1945-11-01), Crawford et al.
patent: 3764384 (1973-10-01), Berni
patent: 3862103 (1975-01-01), Campbell et al.
patent: R27432 (1972-07-01), Torrenzano et al.
Jensen Bruce E.
Tolar Jimmie G.
Air Products and Chemicals Inc.
Bashore S. Leon
Caroff Marc L.
Dannells Richard A.
Moyerman Barry
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