Solvent cleaning and recovery process

Cleaning and liquid contact with solids – Processes – Including regeneration – purification – recovery or separation...

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134 13, 134 22R, 134 38, 203 47, 203 48, 210 42R, B08B 308, B08B 310

Patent

active

040090485

ABSTRACT:
Vinyl halide polymers are removed from the internal surfaces of reaction equipment with a solvent and the solvent recovered by: (1) contacting the polymer-containing solvent with steam forming a slurry; (2) cooling the slurry to form a crumbly precipitate; (3) separating the resulting slurry into an aqueous solvent and a precipitate; (4) adding water to the precipitate to form a second slurry; and (5) separating the second slurry into a second aqueous solvent solution and vinyl halide polymers. The aqueous solvent solutions are dehydrated before being reused in solvent cleaning.

REFERENCES:
patent: 2389958 (1945-11-01), Crawford et al.
patent: 3764384 (1973-10-01), Berni
patent: 3862103 (1975-01-01), Campbell et al.
patent: R27432 (1972-07-01), Torrenzano et al.

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