Manufacturing fluid including fluorescent dye penetrant and...

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Reexamination Certificate

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C252S301500

Reexamination Certificate

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06677584

ABSTRACT:

FIELD OF THE INVENTION
This invention relates to a manufacturing fluid containing a fluorescent dye and method of use for detecting defects in components undergoing machining operations and further relates to ceramic components formed by the manufacturing process.
BACKGROUND OF THE INVENTION
The use of a coatable material to detect defects in the surface of an object is well known as illustrated for example in U.S. Pat. No. 3,777,143 to Winans et al. which discloses an aqueous solution that can be coated onto the surface, dried and partially removed except for a coating retained by surface openings and flaws. Such coatings and methods of using the coating are known generally as “liquid penetrant inspection.” Among the many advantages of these techniques are their non-destructive nature and their ability to allow optical detection of minute surface defects that could not otherwise be optically detected.
Development of liquid penetrant inspection systems and techniques have focused on a variety of different approaches. For example, in U.S. Pat. No. 3,652,224 to Johnson et al. a method is disclosed for enlarging the cracks via a process of corrosion in order to allow the cracks to be detected by conventional penetrating dye liquid. In U.S. Pat. No. 3,981,185 to Molina a system and method is disclosed for applying a dye penetrant, such as a fluorescent dye, that may be applied in a more or less conventional manner followed by the application or a emulsifier to treat the penetrant covered surface to remove the excess penetrant without removing dye penetrant from the cracks and flaws. While this process simplifies the steps involved in removing the excess penetrant, considerable time and expense can still be involved in performing the type of process steps disclosed in this patent.
Still further innovation in liquid penetrant inspection systems has occurred in the composition of the penetrant. For example, U.S. Pat. No. RE 28,605 to Alburger discloses a penetrant containing a solvent ingredient which acts to provide a low degree of emulsifiability to provide improved reliability of flaw indications. U.S. Pat. No. 4,172,224 to Lapinski discloses the concept of using silver nitrate solution to allow detection of microcracks. None of these improved compositions or processes has fully addressed the need for simplifying the steps and costs of employing the resulting liquid penetrant inspection process to make it generally attractive and cost effective.
Development of a variety of different applications or unique delivery systems or techniques have allowed the liquid penetrant inspection concept to be applied to specific environments or problems. For example, U.S. Pat. No. 4,621,193 to Van Hoye discloses a crack detection system including a novel applicator for delivering a fluorescent dye penetrant to provide a more effective system for detecting minute surface flaws. The patent to Tomasch (U.S. Pat. No. 5,115,136) discloses an inspection system which enables the operator to detect minute cracks and flaws in normally inaccessible places of manufactured parts. Still these approaches do not solve the problem of making liquid penetrant inspection cost effective across a broad range of applications.
Liquid penetrant inspection has the potential for broad application as demonstrated in U.S. Pat. No. 4,400,618 to Bupp et al. which discloses a fluorescing dye method for detecting flaws in printed circuit boards. The patent to Alburger (U.S. Pat. No. 3,184,596) is notable for its disclosure of a liquid penetrate inspection system including a detection method that uses fluorescent color dye penetrant to detect minute porosities or fracture cracks in ceramic parts using an ultraviolet light (see col. 1, lines 8-14 and col. 2, lines 70-71). U.S. Pat. No. 4,331,871 to Allinikov discloses a method for detecting flaws in the surface of a workpiece such as engine parts where a fluorescent dye is used to highlight the flaws which may be inspected under an ultraviolet light (see col. 2, lines 47-62).
Ceramic materials have a number of properties that make them extremely useful in applications demanding close tolerances, long operating life and insensitivity to high temperature environments. One particularly important commercial application has been as a component in a high pressure fuel system for diesel engines as disclosed in commonly assigned U.S. Pat. No. 5,899,383. This application requires a material that is capable of operating under very demanding conditions of high pressure (15,000 to 20,000 psi and above) and high temperature. In addition, diesel fuel systems demand components that can operate over extensive periods while in contact with diesel fuel which has low lubricity properties and which may include abrasive particles that cause high failure rates when metal plungers are used.
As disclosed in U.S. Pat. No. 5,899,383, plungers made of certain types of ceramic material have been shown to have unexpectedly favorable operating characteristics in high pressure fuel systems. However, to achieve these operating characteristics the ceramic plunger must be formed to very exacting dimensions and must be essentially defect free. To form ceramic plungers having these characteristics requires the plungers to be subjected to grinding operations. Typically, conventional water-based grinding coolant or cutting fluids are used to allow the grinding operation to achieve the required shape and dimensions.
Acceptable plungers must have sharp edges. This gives rise to a tendency in a relatively small percentage of plungers (e.g. 1 in a 1000) to the formation of chips and closed cracks that are difficult to detect optically. Fluorescent dye penetrant can be used to highlight these defects but use of this technique requires the ceramic plunger to be subjected to a number of additional handling steps that increase the cost of manufacture.
While the compositions, processes and applications disclosed in the prior art may be suitable to achieve their disclosed purposes, no disclosure has been made of a system that is entirely satisfactory in achieving the broad objectives of effectiveness, low cost and efficiency.
SUMMARY OF THE INVENTION
It is a primary object of this invention to overcome the deficiencies of the prior art by providing a fluorescent penetrant system that is substantially more effective, low in cost and more efficient than are the systems disclosed in the prior art.
Another object of the subject invention is to provide a method for forming a component using a manufacturing fluid which facilitates formation and inspection of the component including the steps of adding a fluorescent dye to the manufacturing fluid, subjecting the component to a forming step using the manufacturing fluid including the fluorescent dye, and inspecting the component for surface cracks or defects following the forming step.
Yet another object of the subject invention is to provide a method as described above wherein the forming step includes the step of cutting the component material while applying the manufacturing fluid containing the fluorescent dye.
Still another object is to provide a method for grinding a ceramic material while applying the manufacturing fluid containing the fluorescent dye.
Another object of the invention is to provide a method as described above wherein the manufacturing fluid is an aqueous coolant/lubricant and wherein the fluorescent dye is present in the manufacturing fluid in a dilution range of 1 to 5 parts per 10,000 parts of water.
Another object of the invention is to provide a method as described above wherein the step of providing fluorescent dye includes the step of adding the fluorescent dye to a concentration of between 125 to 500 parts per million.
Still another object of the invention is to provide a method as described above wherein the step of providing fluorescent dye includes the step of adding the fluorescent dye to a concentration of approximately 250 parts per million.
Yet another object is to provide a method as described above wherein the fluorescent dye is DUBL-CHECK A-416

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