Glass manufacturing – Processes – With chemically reactive treatment of glass preform
Reexamination Certificate
2000-02-22
2003-04-29
Resan, Stevan A. (Department: 1773)
Glass manufacturing
Processes
With chemically reactive treatment of glass preform
C065S088000, C216S097000, C216S100000, C216S103000, C216S104000, C216S108000, C216S109000
Reexamination Certificate
active
06553788
ABSTRACT:
BACKGROUND OF THE INVENTION
The present invention relates to a glass substrate and a method of manufacturing a glass substrate, and more particularly, to a glass substrate and manufacturing method for a magnetic disk, which has a fine textured surface.
Magnetic disks for use in hard disk drives are typically formed with a fine textured surface (pits and projections) for preventing adhesion between a head and the magnetic disk surfaces. In recent years, finer textures have been desired in order to increase the density of magnetic recording. However, using commercially practiced film texture methods and mechanical texture methods it is difficult to form the required fine textured surfaces.
Some techniques for forming a texture on the surfaces of substrates through etching are known. For example, Japanese Unexamined Patent Publication No. Hei 5-314456 discloses a technique for forming a texture by etching a glass substrate in a mixed solution of hydrofluoric acid and potassium fluoride. Japanese Unexamined Patent Publication No. Hei 10-134348 discloses a technique for forming a magnetic layer and a protective layer on a glass substrate in sequence, and then forming a texture on the surfaces of the protective layer through etching. The texture formed by the above prior art has a maximum surface roughness Rmax of 30 angstroms.
Japanese Unexamined Patent Publication No. Hei 7-153059 discloses a technique for forming a texture directly on surfaces of a glass substrate by etching the glass substrate in a hydrofluoric acid-potassium fluoride mixed solution. The height of projections of the resulting texture ranges from 130 to 400 angstroms when measured by a contact needle type surface roughness tester (trade name: Taristep, manufactured by Lank Taylor Bobson Co.).
However, the glass substrates fabricated by the prior art may sometimes have localized areas with higher projections than the average height of projections, which is known as an asperity. If a magnetic disk is manufactured using the glass substrate having such asperity, the resulting magnetic disk may experience head crash. Such a magnetic disk is susceptible to a gliding error, which may arise when a magnetic head hits an asperity in its movement (gliding). Thus, the asperity reduces production yields of the magnetic disks.
Also, even if glass substrates having the same composition are etched under the same conditions, the roughness and configuration of the fine textured surface cannot be consistently reproduced. Such unstable reproducibility makes it difficult to reliably mass-produce glass substrates having uniformly fine textures.
In recent years, majority type of hard disk drives is a ramped loading type. The magnetic head, which used in the ramped loading type, is located above the disk surface spaced by about 10 nm. However, the design of magnetic heads differs from one hard-disk manufacturer to another, also the design of head-disk-interfaces differs. Therefore, the hard-disk manufacturers respectively require slightly different degrees of surface roughness on the magnetic disk. It is therefore desired to accurately control the roughness of the fine textured surfaces.
SUMMARY OF THE INVENTION
It is an object of the present invention to provide a method of manufacturing substrates, which is capable of forming a fine texture without asperity with good reproducibility.
To achieve the above objective, the present invention provides a method for manufacturing a glass substrate for a magnetic disk. The method includes scrub-etching a surface of a glass substrate material using a scrubbing pad in the presence of an acid treatment solution.
Another aspect of the present invention provides a glass substrate for a magnetic disk including a glass substrate material having a fine texture formed on a surface thereof by scrub-etching.
Further aspect of the present invention provides a method of manufacturing a substrate for a magnetic disk. The method includes forming a fine texture, having an average surface roughness Ra in a range between 0.4 and 3.0 nm and a ratio of a 10-points mean roughness (Rz) to the average surface roughness Ra of 14 or less, on a substrate made of an inorganic material or on a substrate having an alloy film on a surface thereof. The forming step includes the repeatedly performing an immersion process or scrub process several times using an acid solution under different conditions.
Further aspect of the present invention provides a substrate for a magnetic disk having a fine texture. The substrate has an average surface roughness Ra in a range of 0.4 to 3.0 nm and a ratio of a 10-points mean roughness Rz to the average surface roughness Ra equal to or less than 14.
Other aspects and advantages of the present invention will become apparent from the following description, taken in conjunction with the accompanying drawings, illustrating by way of example the principles of the invention.
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Ikeda Hiroshi
Matsuno Yoshihiro
Watanabe Takeo
Marsh & Fischmann & Breyfogle LLP
Nippon Sheet Glass Co. Ltd.
Resan Stevan A.
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