Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acid esters
Patent
1988-11-02
1990-10-02
Shippen, Michael L.
Organic compounds -- part of the class 532-570 series
Organic compounds
Carboxylic acid esters
C07C10366
Patent
active
049609238
ABSTRACT:
The process for preparing a novel product, pure crystalline methyl 2-acryloylamino-2-methoxyacetate, involves reacting pure crystalline, anhydrous acrylamido-glycolic acid in an anhydrous medium with methanol in the presence of hydrogen chloride. This is subsequently neutralized with an alkali metal bicarbonate, and then the mineral salts are filtered off. Finally, pure crystalline methyl 2-acryloylamino-2-methoxyacetate is obtained by taking up the concentrated reaction medium in 1,1,1-trichloroethane under vacuum.
REFERENCES:
patent: 4443623 (1984-04-01), Photis
patent: 4760168 (1988-07-01), Schirmann
Christidis Yani
Sidot Christian
Shippen Michael L.
Societe Francaise Hoechst
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