Recrystallization of hexsanitrostilbene from nitric acid and wat

Details Recrystallization of hexsanitrostilbene from nitric acid and wat Recrystallization of hexsanitrostilbene from nitric acid and wat

1980-03-03

1981-04-07

Sebastian, Leland A.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

C07C 7910

Patent

active

042608376

ABSTRACT:
The production of 2,2',4,4',6,6'-hexanitrostilbene-I (HNS-I) having finely ivided particles of uniform size by dissolving HNS-II in hot fuming nitric acid and then drowning the HNS-nitric acid solution in water.

REFERENCES:
patent: 3201481 (1965-08-01), Catino et al.
patent: 3505413 (1970-04-01), Shipp
patent: 3699176 (1972-10-01), Syrop
patent: 4085152 (1978-04-01), Salter et al.
O'Keefe, Chem. Abs., vol. 87, 186685h (1977).

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