Vitamin D compounds isotopically substituted at carbon 6 and pro

Details Vitamin D compounds isotopically substituted at carbon 6 and pro Vitamin D compounds isotopically substituted at carbon 6 and pro

1980-07-17

1981-10-27

Roberts, Elbert L.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07J 900

Patent

active

042972892

ABSTRACT:
A method for isotopically labeling carbon-6 of vitamin D and 5,6-trans-vitamin D compounds which comprises reducing the corresponding 6-oxo-cyclovitamin with a tritio- or deutero-borohydride and subjecting the reduction product to acid-catalyzed solvolysis.
The 6-labeled compounds find application in the elucidation of vitamin D metabolism and function and in vitamin metabolite analyses.

REFERENCES:
patent: 4195027 (1980-03-01), DeLuca et al.
patent: 4224231 (1980-09-01), DeLuca et al.

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