Synthesis of ordered mesoporous carbon-silicon nanocomposites

Chemistry of inorganic compounds – Silicon or compound thereof – Binary compound

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C423S345000, C423S439000, C502S178000, C501S088000, C264S624000, C264S625000, C264S628000, C264S682000, C977S882000, C977S883000

Reexamination Certificate

active

07910082

ABSTRACT:
A method for preparing ordered mesoporous silicon carbide (OMSiC) nanocomposites uses an evaporation-induced self-assembly of a precursor composition that preferably includes a phenolic resin, pre-hydrolyzed tetraethyl orthosilicate, a surfactant, and butanol. The precursor mixture is dried, cross-linked and heated to form ordered mesoporous silicon carbide material having discrete domains of ordered, mesoscale pores.

REFERENCES:
patent: 6001756 (1999-12-01), Takahashi et al.
patent: 7056849 (2006-06-01), Wan et al.
patent: 7087656 (2006-08-01), Garcia et al.
patent: 7419772 (2008-09-01), Watkins et al.
patent: 7648932 (2010-01-01), Weisensel et al.
patent: 7807267 (2010-10-01), Kohmura et al.
patent: 2005/0084717 (2005-04-01), Tani et al.
patent: 2006/0110308 (2006-05-01), Gupta et al.
patent: 2007/0042268 (2007-02-01), Pak et al.
patent: 2008/0152577 (2008-06-01), Addiego et al.
patent: 2008/0220244 (2008-09-01), Wai et al.
patent: 2008/0317953 (2008-12-01), Watkins et al.
patent: 1401564 (2003-03-01), None
patent: 09-048605 (1997-02-01), None
patent: 2007261882 (2007-10-01), None
patent: 9937705 (1999-07-01), None
patent: 2010/019229 (2010-02-01), None
“Morphology-Controlled Synthesis of Nanostructured Silicon Carbide,” Xiang-Yun Guo et al. Materials Research Society, vol. 815 (2004), pp. J5.3.1 to J5.3.6.
“Preparation of Ordered Mesoporous SiC from Perceramic Polymer Templated by Nanoporous Silica,” Jia Yan et al. J. Phys. Chem. B (2006), 110, pp. 5429-5433.
“Ordered Mesoporous silicon carbide (OM-SiC) via polymer precursor nanocasting,” Piotr Krawiec et al. The Royal Society of Chemistry 2006 (Chem. Commun.,), pp. 2469-2470.
“Periodic mesoporous organosilica mesophates are versatile precursors for the direct preparation of mesoporous silica/carbon composites, carbon and silicon carbide materials,” Zhuxian Yang et al. J. Mater. Chem., 2006, 16, pp. 3417-3425.
“Highly Ordered Mesoporous Silicon Carbide Ceramics with Large Surface Areas and High Stability,” Yifeng Shi et al. Advanced Functional Materials, 2006, 16, pp. 561-567.
“Direct Preparation of High Surface Area Mesoporous SiC-based Ceramic by Pyrolysis of a Self-Assembled Polycarbosilane-block-Polystyrene Diblock Copolymer,” Quoc Dat Nghiem et al. Chem. Mater. 2008, 20, pp. 3735-3739.
“Synthesis and characterization of mesoporous silicon carbide,” Guo-Qiang Jin et al. Microporous and Mesoporous Materials 60 (2003), pp. 207-212.
Raman et al.; “Synthesis of silicon carbide nanorods from mixture of polymer and sol-gel silica”; J Mater Sci (2007) 42: 5891-5895.
Vix-Guterl et al.; “Effect of the properties of a carbon substrate on its reaction with silica for silicon carbide formation”; Carbon vol. 35, No. 10-11, pp. 1587-1592, 1997.
Shi et al.; “Highly ordered mesoporous silicon carbide ceramics with large surface areas and high stability”; Adv. Funct. Mater. 2006, 561-567.
Krawiec et al,; “Ordered mesoporous silicon carbide (OM-SiC) via polymer precursor nanocasting”; The Royal Society Of Chemistry, 2006, 2469-2470.
Shi et al.; “Ordered mesoporous SiOC and SiCN ceramics from atmosphere-assisted in situ transformation”; Chem. Mater. 2007, 19, 1761-1771.
Yao et al.; “Rode of pores in the carbothermal reduction of carbon-silica nanocomposites into silicon carbide nanostructures”; J. Phys. Chem. C 2007, 111, 636-641.
Vix-Guterl et al.; “SiC material produced by carbothermal reduction of a freeze gel silica-carbon artefact”; Journal of the European Ceramic Society 19 (1999), 427-432.
Yan et al.; “Preparation of ordered mesoporous SiCN ceramics with large surface area and high thermal stability”; Microporous and Mesoporous Materials 100 (2007) 128-133.
Besson et al.; “Highly ordered orthorhombic mesoporous silica films”; Microporous and Mesoporous Materials 60 (2003) 43-49.
Schwetz; “Handbook of ceramic hard materials”; ed. R. Riedel, Wiley-VCH, Weinheim, 2000, vol. 1, pp. 683-748.
Lu et al.; “High surface area mesoporous SiC synthesized via nanocasting and carbothermal reduction process”; Journal of Materials Science (2005).
Krawiec et al.; “SiC/MCM-48 and SiC/SBA-15 nanocomposite materials”; Chem. Mater. 2004, 16, 2869-2880.
Park et al.; “A facile route to prepare high surface area mesoporous SiC from SiO2 sphere templates”; J. Mater. Chem., 2004, 14, 3436-3439.
Feng et al.; “Control of pore sizes in mesoporous silica templated by liquid crystals in block copolymer-cosurfactant-water systems”; Langmuir 2000, 16, 5304-5310.
Piotr Krawiec, et al “Tubular and Rodlike Ordered Mesoporous Silicon (Oxy)carbide Ceramics and their Structural Transformation,” chem.. Mater. 2008, 20, 5421-5433.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Synthesis of ordered mesoporous carbon-silicon nanocomposites does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Synthesis of ordered mesoporous carbon-silicon nanocomposites, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Synthesis of ordered mesoporous carbon-silicon nanocomposites will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-2649076

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.