Production of diethanolamine

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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C07C21300

Patent

active

060639652

ABSTRACT:
This invention concerns a process for preparation of alkanolamines such as diethanolamine (DEA) from ammonia and an alkylene oxide such as ethylene oxide. The yield of DEA may be increased by adding monoethanolamine (MEA) to the second feed in a split feed reactor scheme. The process can be conducted as a multistep process, such as by reacting a portion of the ethylene oxide followed by addition of a second charge of ethylene oxide after complete reaction of the first charge of ethylene oxide.

REFERENCES:
McMillan, Thomas I., "Ethylene Oxide Derivatives" SRI International Report No. 193, Private Report by the Process Economics Program, Jan. 1991.

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