Method of preparing tetraalkyl thiuram disulfides

Details Method of preparing tetraalkyl thiuram disulfides Method of preparing tetraalkyl thiuram disulfides

1977-12-14

1979-03-13

Chan, Nicky

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C15510

Patent

active

041442725

ABSTRACT:
Method of preparing tetraalkyl thiuram disulfides by racting a secondary amine with carbon disulfide in a substantially neutral solution of a saturated aliphatic alcohol and oxidizing the dithiocarbamate formed thereby with a hydroperoxide. The invention has particular utility by providing a relatively pollution-free method of preparing tetraalkyl thiuram disulfides.

REFERENCES:
patent: 1413172 (1922-04-01), Lorentz
patent: 1782111 (1930-11-01), Adams

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