Chemistry of inorganic compounds – Silicon or compound thereof – Oxygen containing
Patent
1976-06-25
1978-05-09
Meros, Edward J.
Chemistry of inorganic compounds
Silicon or compound thereof
Oxygen containing
423328, C01B 3328
Patent
active
040887391
ABSTRACT:
An improved process for preparing synthetic ferrierites having the absorption and catalytic properties characteristic of 5 to 8 angstrom zeolites which comprises promoting an alkaline reaction mixture comprising Group I and/or Group II cations, a source of silica, a source of alumina with lithium cations. The promoted reaction mixture is seeded with natural or synthetic ferrierite seeds, and heated to convert the mass to the synthetic ferrierite.
The product has the empirical formula, 0.1 to 0.9 Li.sub.2 O:0.1:0.9 R.sub.2 0:Al.sub.2 O.sub.3 :6 to 25 SiO.sub.2 wherein R.sub.2 O is Na.sub.2 O, K.sub.2 O, or Rb.sub.2 O and/or Cs.sub.2 O; 0.1 to 0.9 Li.sub.2 O:0.1 to 0.9 WO:Al.sub.2 O.sub.3 :6 to 25 SiO.sub.2 wherein WO is BaO, CaO, MgO or SrO; or (Li.sub.2 O:R.sub.2 O:WO):Al.sub.2 O.sub.3 :6-25 SiO.sub.2 where R.sub.2 O is any R.sub.2 O above and WO is any WO above.
REFERENCES:
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Barrer et al. "Chemical Society Journal" 1964, Pt. 1, pp. 485-497.
Alietti et al. "The American Mineralogist" vol. 52, 1967, pp. 1562 & 1563.
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Barrer et al., "The American Mineralogist" vol. 50, Mar.-Apr., 1965, pp. 484-489.
Wise et al., "The American Mineralogist" vol. 54, 1969, pp. 887-895.
Edwards Grant C.
Vaughan David E. W.
McDowell, Jr. William W.
Meros Edward J.
Savage Arthur P.
W. R. Grace & Co.
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