Process for the production of 5-bromo-5-nitro-1,3-dioxane

Details Process for the production of 5-bromo-5-nitro-1,3-dioxane Process for the production of 5-bromo-5-nitro-1,3-dioxane

1973-09-13

1976-01-06

Milestone, Norma S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D31906

Patent

active

039312330

ABSTRACT:
An improved process for the production of 5-bromo-5-nitro-1,3-dioxane by the acetalization of formaldehyde with 2-bromo-2-nitro-propanediol-1,3 in the presence of concentrated sulfuric acid as a catalyst and recovery of readily crystallizable 5-bromo-5-nitro-1,3-dioxane.

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