Purification method for prolyl-leucylglycinamide

Details Purification method for prolyl-leucylglycinamide Purification method for prolyl-leucylglycinamide

1974-10-31

1976-01-06

Gotts, Lewis

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C10352, C07G 700

Patent

active

039311848

ABSTRACT:
The tripeptide L-prolyl-L-leucylglycinamide can be obtained in pure, crystalline form by dissolving it in methanol and adding to a clear methanol solution thereof, a relatively large volume of diethyl ether. The obtained tripeptide shows essentially only a single spot on TLC plates.

REFERENCES:
patent: 3708593 (1973-01-01), Plotnikoff
patent: 3795738 (1974-03-01), Plotnikoff
Nair et al.: Biochem. Biophys. Res. Comm., 43, 1376-1381 (1971).

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