Production of urea fluorosilicate

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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C07C12701

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active

H00006769

ABSTRACT:
A process for producing urea fluorosilicate, [(NH.sub.2).sub.2 CO].sub.4 .multidot.H.sub.2 SiF.sub.6, a composition eminently suitable for use as a fungicide in the prevention and control of wheat stem rust. The method involves mixing urea and fluorosilicic acid derived from by-product fluorine in a mole ratio of urea:fluorosilicate acid in the range from about 3.5:1 to about 4.5:1 and thereafter dewatering the resulting solution to produce a concentrated solution of urea fluorosilicate. Solid urea fluorosilicate is subsequently obtained by evaporation of the remaining water which is conveniently effected by introducing the resulting solution or melt to concentrator means, or alternatively into a heated, moving bed of preformed granular urea fluorosilicate.

REFERENCES:
patent: 4461913 (1984-07-01), Lewis et al.

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