Method and apparatus for evaporating and separating multiple com

Liquid purification or separation – Constituent mixture variation responsive – With membrane

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Details

159 27A, 159 31, 159 44, 202200, 210 71, 210 73R, 210110, 210182, 210258, B01D 112

Patent

active

039650057

ABSTRACT:
Apparatus for separating feed solution, such as chrome or nickel plating rinse solutions, into a concentrated liquor portion and a solvent portion, comprising vertical shell and tube evaporator means for generating a stream of vapor and entrained droplets; first impingement means for separating a first liquor portion from the stream; second impingement means for separating a second liquid portion from the stream; mesh entrainment pad means for separating a third liquor portion from the stream to form a stream consisting essentially of pure solvent vapor; reduced pressure generating means for drawing the stream from the evaporator tubes through the impingement and mesh entrainment pad; capacitance means for accumulating a preselected volume of the first, second, and third liquor portions above the lower end of the evaporator; and conduit means for recycling liquor from the capacitance means to the evaporator means. The apparatus includes a shell and tube evaporator and an especially efficient impingement member, and the process steps for operating said apparatus to separate feed solution into an essentially pure solvent such as distilled water and a liquor of a preselected concentration are described.

REFERENCES:
patent: 1436739 (1922-11-01), Webre
patent: 1883379 (1932-10-01), Kermer
patent: 1943106 (1934-01-01), Burnham
patent: 2199320 (1940-04-01), Von Le Juge
patent: 2628168 (1953-02-01), Madsen
patent: 2745484 (1956-05-01), Eckstrom et al.
patent: 2768813 (1956-10-01), Boyer
patent: 2800955 (1957-07-01), Honig et al.
patent: 3203466 (1965-08-01), Eckstrom
patent: 3686077 (1972-08-01), De Koning

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