Chemistry of inorganic compounds – Modifying or removing component of normally gaseous mixture – Carbon dioxide or hydrogen sulfide component
Patent
1979-08-08
1981-02-17
Thomas, Earl C.
Chemistry of inorganic compounds
Modifying or removing component of normally gaseous mixture
Carbon dioxide or hydrogen sulfide component
423541R, 423557, 252411S, B01D 5334
Patent
active
042514959
ABSTRACT:
Process for purifying a gas containing hydrogen sulfide, optionally with carbon dioxide, particularly adapted to the purification of gases of relatively low hydrogen sulfide content, e.g. not in excess of 1% of H.sub.2 S by volume, comprising contacting the gas with an absorption mass containing copper, at a temperature of from 250.degree. to 550.degree. C., to absorb the hydrogen sulfide and form copper sulfide; wherein the absorption mass is regenerated by interrupting the contact of the gas with the mass when the mass is at least partially saturated, contacting the mass with an oxidizing gas containing from 0.5 to 5% by volume of oxygen, at a temperature of from 250.degree. to 345.degree. C., to convert the copper sulfide substantially to copper sulfate, and then contacting the mass with a reducing gas containing from 5 to 20% by volume of hydrogen, at a temperature of from 300.degree. to 450.degree. C., to convert the copper sulfate substantially to sulfur dioxide and metallic copper, thereby regenerating the mass, which is then contacted again by the hydrogen sulfide containing gas.
REFERENCES:
patent: 2747968 (1956-05-01), Pigache
patent: 3079223 (1963-02-01), Lewis
patent: 3778501 (1973-12-01), Lang et al.
patent: 4008174 (1977-02-01), Jacobson et al.
Deschamps Andre
Franckowiak Sigismond
Sugier Andre
Institut Francais du Pe'trole
Thomas Earl C.
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