Process for the production of terephthalic acid

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof

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562485, 562486, 562487, C07C 5116

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active

055279570

ABSTRACT:
A terephthalic acid slurry in acetic acid is produced by oxidizing p-xylene in acetic acid, removing water by evaporation of a stream of water and acetic acid, and returning acetic acid to the oxidation step. The terephthalic acid is separated from the reaction medium in a first zone to leave a deposit on a band, the deposit is washed with a first aqueous medium in a second zone, removed from the band in a third zone, and admixed with a second aqueous medium. Reaction medium is passed from the first zone to the oxidation step and terephthalic acid is recovered, preferably after further purification.

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"Filtration and Gegenstromwaschung auf dem Vakuumbandfilter", Kuhlen, cav, Apr. 1983.

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