Separation of 3-methyl-1-butanol from 1-pentanol by extractive d

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

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203 44, 203 46, 203 57, 203 59, 203 60, 203 62, 203 68, C07C 2732

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active

057636958

ABSTRACT:
3-Methyl-1-butanol cannot be separated from 1-pentanol by distillation or rectification because of the closeness of their boiling points. 3-Methyl-1-butanol is readily separated from 1-pentanol by extractive distillation. Effective agents are butyl benzoate, 2-undecanone and diethylene glycol methyl ether.

REFERENCES:
patent: 2552911 (1951-05-01), Steitz
patent: 2635072 (1953-04-01), Eliot
patent: 4969977 (1990-11-01), Berg

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