Method for purification of 1,1,1,2-tetrafluoroethane

Organic compounds -- part of the class 532-570 series – Organic compounds – Halogen containing

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570166, 570169, C07C 1738

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active

054441714

ABSTRACT:
In the production of 1,1,1,2-tetrafluoroethane by reacting trichloroethylene with hydrogen fluoride, crude 1,1,1,2-tetrafluoroethane is highly purified by a method comprising subjecting the crude 1,1,1,2-tetrafluoroethane to preliminary purification to remove hydrogen chloride to a concentration of not higher than 2%, and bring the preliminarily purified 1,1,1,2-tetrafluoroethane containing one or more unsaturated impurities and hydrogen fluoride in an amount at least equimolar to the unsaturated impurities into contact with a fluorination catalyst in a vapor phase to decrease the content of the unsaturated impurities.

REFERENCES:
patent: 4158675 (1979-06-01), Potter

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