Synthesis of N-t-butyl-p-menthane-3-carboxamide

Details Synthesis of N-t-butyl-p-menthane-3-carboxamide Synthesis of N-t-butyl-p-menthane-3-carboxamide

1981-04-27

1982-09-21

Demers, Arthur P.

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

C07C103737

Patent

active

043508324

ABSTRACT:
This invention provides an efficient two-step reaction sequence for producing N-t-butyl-p-menthane-3-carboxamide. The process involves forming 3-p-menthylmagnesium halide, and reacting the 3-p-menthylmagnesium halide with t-butyl isocyanate to form the product.

REFERENCES:
patent: 3483248 (1969-12-01), Pattison
patent: 3898078 (1975-08-01), Fitzgerald et al.
patent: 4150052 (1979-04-01), Watson et al.
patent: 4178459 (1979-12-01), Watson et al.
patent: 4193936 (1980-03-01), Watson et al.
patent: 4248859 (1981-02-01), Rowsell et al.
Wagner et al., Synthetic Organic Chemistry, John Wiley & Sons, N.Y., N.Y., 1955, p. 571.
Singleton et al., J.A.C.S. 60, (1938), pp. 540-543.

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