Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...
Patent
1995-04-28
1999-02-16
Trinh, Ba K.
Organic compounds -- part of the class 532-570 series
Organic compounds
Heterocyclic carbon compounds containing a hetero ring...
568463, 568466, C07D32306
Patent
active
058722637
ABSTRACT:
A process for separating a gaseous reaction mixture in the preparation of trioxane is described, in which a) the gaseous mixture leaving the reactor is scrubbed in countercurrent with an organic solvent whose boiling point is above 135.degree. C. in which the trioxane predominantly dissolves and which leaves the formaldehyde predominantly in the gas phase which is returned to the reactor, b) the trioxane together with residual formaldehyde is stripped from the solvent by distillation via a column, the overhead product being partially condensed in the temperature range from 62.degree. to 100.degree. C. c) some of the resulting condensate is applied to the column as reflux and some is taken off as product and d) the non-condensed portion is returned to the scrubbing step a).
REFERENCES:
patent: 2304080 (1942-12-01), Frank
patent: 3496192 (1970-02-01), Ackerman et al.
JP-A 59 25387, English Abstract, 1982.
Hoffmockel Michael
Muck Karl-Friedrich
Sextro Gunter
Hoechst Aktiengesellschaft
Trinh Ba K.
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