Method for making tris(hydroxyphenyl) compounds using ion exchan

Organic compounds -- part of the class 532-570 series – Organic compounds – Acyclic carbon bonded directly to three benzene rings or to...

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C09B 1104

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active

059691670

ABSTRACT:
An improved method for the preparation of tris(4-hydroxyphenyl) compounds is provided. In particular, an improved method for preparing 1, 1, 1-tris(4'-hydroxyphenyl)ethane is provided which comprises heating a mixture comprising phenol and 4-hydroxy acetophenone in the presence of effective amounts of an ion exchange catalyst and a mercaptan as a copromoter such that the resulting 1, 1, 1-tris(4'-hydroxyphenyl)ethane is substantially free of various reaction impurities.

REFERENCES:
patent: 4931594 (1990-06-01), Knebel et al.
patent: 5756781 (1998-05-01), Sybert et al.

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