Process for the manufacture of 7-nitro-1,3,5-triaza-adamantane

Details Process for the manufacture of 7-nitro-1,3,5-triaza-adamantane Process for the manufacture of 7-nitro-1,3,5-triaza-adamantane

1979-07-16

1981-05-12

Ford, John M.

Organic compounds -- part of the class 532-570 series

Organic compounds

Four or more ring nitrogens in the bicyclo ring system

C07D48718

Patent

active

042673224

ABSTRACT:
The invention relates to an improved process for the manufacture of 7-nitro-1,3,5-triaza-adamantane from hexamethylene tetramine and nitromethane, using alcohols or carboxylic acids as solvent the water content of which is not allowed to exceed a defined level. The product of the process is obtained with good yield and a high purity degree.

REFERENCES:
patent: 3301854 (1967-01-01), Gabel
patent: 3575974 (1971-04-01), Hodge
Safar et al., Coll. Czech. Chem. Comm., vol. 40, pp. 2179-2182 (1957).

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