Preparation of nitroesters via the reaction of nitroparaffins wi

Details Preparation of nitroesters via the reaction of nitroparaffins wi Preparation of nitroesters via the reaction of nitroparaffins wi

1988-09-20

1989-10-10

Gray, Bruce

Organic compounds -- part of the class 532-570 series

Organic compounds

Carboxylic acid esters

560 20, 560 21, 560156, C07C 7941

Patent

active

048733580

ABSTRACT:
A process to form alkyl nitroacetates by reacting, in a common solvent and in the presence of a base, a nitroparaffin and a cyanoformate. The desired product is formed by a simple one-step process using inexpensive and readily available reactants.

REFERENCES:
patent: 3761510 (1973-09-01), Sifniades
patent: 4433162 (1984-02-01), Hamamoto et al.
patent: 4495362 (1985-01-01), Honda et al.
Kornblum et al., J. Am. Chem. Soc., 77, 6654 (1955).
Finkseiner et al., J. Org. Chem., 28, 215 (1963).
Zen et al., J. Chem. Soc. of Japan, Ind. Chem. Sec., 74, 70 (1971).
Sifniades, J. Org. Chem., 40, 3562 (1975).
Angew. Chem. Int. 21 139 No. 2 (1982).

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