Process for the preparation of .alpha.,.omega.-bis-fluorosulfato

Details Process for the preparation of .alpha.,.omega.-bis-fluorosulfato Process for the preparation of .alpha.,.omega.-bis-fluorosulfato

1982-07-14

1984-08-21

Chan, Nicky

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

560180, 560184, 204 59F, 204 72, 204 79, C07C14110

Patent

active

044669267

ABSTRACT:
A method for making alpha,omega-bis-fluorosulfatoperfluoroalkanes by reacting a perfluorinated alpha-olefin with peroxodisulfuryl difluoride in the liquid phase, and compounds of the formula

REFERENCES:
patent: 4235804 (1980-11-01), Krespan
Shreeve et al., JACS, 83, 4521 (1961).
Krespan, J. Fluorine Chem. 2, 173-180 (1972/73).
Germain et al., Tetrahedron 37, 487-491 (1981).
Lustig et al., Inorganic Chem. 3, 287-288 (1964).
Chem. Abstr. 93, 238771x (1980).

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