Variable flow capillary gas chromatography method

Measuring and testing – Gas analysis – Gas chromatography

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422 89, G01N 3108

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active

048723347

ABSTRACT:
A method for temperature programmed capillary column gas chromatography characterized in that carrier gas is flowed in an amount greater than that under normal separation conditions for a term starting from before injection of a sample or immediately after the injection and ending at any time point from immediately after a solvent in the sample commences to enter into a column to the solvent finishing passing through the column. The invention is also apparatus for the above method characterized in that the apparatus has two flow paths for carrier gas which, for example, join to one flow path before a sample injection device, and one of the flow paths has a valve which can rapidly stop or decrease the flow of the carrier gas in that flow path.

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